Differences

This shows you the differences between two versions of the page.

--- crystallography:collection:frx:on [2016/07/25 09:41] – created bonnefon
+++ crystallography:collection:frx:on [2023/11/01 20:19] (current) – external edit 127.0.0.1
@@ Line 1: / Line 1: @@
 Turn ON FR-X
-===== Turn in-house FR-X OFF =====
+===== Turn in-house FR-X ON =====
 ----
-==== Engine Room ====
+==== Technical Room E0044 ====
-Switch ON the main switch of the water cooling device in the engine room.
+Turn the tap on the main water inlet to the ON position.
+{{:crystallography:collection:frx:red_valve.jpg?400|}}
+Switch ON the water chiller (HASKRIS) using the main switch only.
 Wait until the temperature is stabilized at 17°C.
+{{:crystallography:collection:frx:haskins.jpg?200|}}
+{{:crystallography:collection:frx:haskins_closeup.jpg?400|}}
-Switch ON the nitrogen compressor in the engine room using the touch panel.
+Switch ON the nitrogen compressor at the back, then start the nitrogen flow with the touch panel.
 After a 3 min idle wait, the pump should stabilize in 30 min.
 Wait for 1 h.
+{{:crystallography:collection:frx:n2.jpg?150|}}
+{{:crystallography:collection:frx:n2_closeup.jpg?400|}}
+----
 ==== FR-X ====
-Switch the main power source ON.
+Switch ON the two fans of AFC-11.
-Reset and then switch ON at the back of the FR-X.
+{{:crystallography:collection:frx:acf11_back.jpg?400|}}
-POWER ON on the FR-X main panel.
+Switch ON AFC-11 Goniometer controller.
-Start the Vacuum on the XG Control panel. Wait until vacuum is below 1.10E-4 (about 1h30).
+{{:crystallography:collection:frx:afc11_closeup.jpg?600|}}
-Decrease gradually the voltage and intensity from 45 kV and 66 mA to 20 kV and 10 mA. First step 66->60 mA, then 45->40 kV. Wait 10 s. Then decrease by steps of 10. (Lower the intensity first)
+Switch ON the vacuum pump below the Cobra Controller.
-Turn X-RAY OFF on the XG Control panel. Wait 1h.
+{{:crystallography:collection:frx:pump1.jpg?250|}}
+{{:crystallography:collection:frx:pump1_closeup.jpg?250|}}
+Switch ON the vacuum pump below the BioSAXS.
+{{:crystallography:collection:frx:pump2.jpg?250|}}
+{{:crystallography:collection:frx:pump2_closeup.jpg?350|}}
+Switch ON the transformer.
+{{:crystallography:collection:frx:main_power_supply.jpg?600|}}
+Reset and then switch ON the generator at the back.
+{{:crystallography:collection:frx:frx_back.jpg?400|}}
+POWER ON on the front main panel.
+Press both DOOR LOCK buttons.
+{{:crystallography:collection:frx:frx_front.jpg?600|}}
+Start the Vacuum on the XG Control panel.
+Wait until vacuum is below 1.10E-4 (about 1h30).
+{{:crystallography:collection:frx:xg.png?600|}}
+Turn X-Rays ON on the XG Control panel.
+Wait 1-2h if it was down for a few hours (heating will generate gaz that may disrupt the vacuum if the level is not low enough). Wait overnight if it was down for a few weeks.
+Start the AGING procedure.
+Short aging lasts 31 min, long aging lasts 6h.
+Wait 1h30 for the beam to stabilize before data collection.
 ----
@@ Line 39: / Line 75: @@
 ==== Cryostream ====
-Program / Ramp (change with dial) / Enter
+Switch ON the helium compressor.
-Choose the speed (up to 360K/h) / Enter
+{{:crystallography:collection:frx:helium.jpg?300|}}
-Target / Ambient / Enter
+{{:crystallography:collection:frx:helium_back.jpg?250|}}
-Enter / Enter
-Start
-When ambient temperature is reached, stop
+Switch ON on the back of the device.
-Turn OFF at the back
+{{:crystallography:collection:frx:cobra_back.jpg?600|}}
+Cycle Start/Start
+For the first hour the temperature won't really decrease much.
+Final temperature should be around 100 K.
+{{:crystallography:collection:frx:cobra_front.jpg?600|}}
 ----
+==== Detector ====
+Switch ON the EIGER water chiller.
+{{:crystallography:collection:frx:eiger_chiller.jpg?400|}}
+Switch ON the power supply for the EIGER.
+{{:crystallography:collection:frx:eiger_power_supply.jpg?600|}}
+Switch ON the framegrabber.
+{{:crystallography:collection:frx:framegrabber.jpg?600|}}