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crystallography:collection:frx:on [2016/07/25 09:48] bonnefoncrystallography:collection:frx:on [2023/11/01 20:19] (current) – external edit 127.0.0.1
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 Turn ON FR-X Turn ON FR-X
  
-===== Turn in-house FR-X OFF =====+===== Turn in-house FR-X ON =====
  
 ---- ----
  
-==== Engine Room ====+==== Technical Room E0044 ====
  
-Switch ON the main switch of the water cooling device in the engine room.+Turn the tap on the main water inlet to the ON position. 
 + 
 +{{:crystallography:collection:frx:red_valve.jpg?400|}} 
 + 
 +Switch ON the water chiller (HASKRIS) using the main switch only.
 Wait until the temperature is stabilized at 17°C. Wait until the temperature is stabilized at 17°C.
  
 +{{:crystallography:collection:frx:haskins.jpg?200|}}
 +{{:crystallography:collection:frx:haskins_closeup.jpg?400|}}
  
-Switch ON the nitrogen compressor in the engine room using the touch panel.+Switch ON the nitrogen compressor at the back, then start the nitrogen flow with the touch panel.
 After a 3 min idle wait, the pump should stabilize in 30 min. After a 3 min idle wait, the pump should stabilize in 30 min.
-Wait for 1 h. +Wait for 1 h. 
 + 
 +{{:crystallography:collection:frx:n2.jpg?150|}} 
 +{{:crystallography:collection:frx:n2_closeup.jpg?400|}} 
  
 ---- ----
Line 19: Line 28:
 ==== FR-X ==== ==== FR-X ====
  
-Switch the main power source ON.+Switch ON the two fans of AFC-11.
  
-Reset and then switch ON at the back of the FR-X.+{{:crystallography:collection:frx:acf11_back.jpg?400|}}
  
-POWER ON on the FR-X main panel.+Switch ON AFC-11 Goniometer controller. 
 + 
 +{{:crystallography:collection:frx:afc11_closeup.jpg?600|}} 
 + 
 +Switch ON the vacuum pump below the Cobra Controller. 
 + 
 +{{:crystallography:collection:frx:pump1.jpg?250|}} 
 +{{:crystallography:collection:frx:pump1_closeup.jpg?250|}} 
 + 
 +Switch ON the vacuum pump below the BioSAXS. 
 + 
 +{{:crystallography:collection:frx:pump2.jpg?250|}} 
 +{{:crystallography:collection:frx:pump2_closeup.jpg?350|}} 
 + 
 +Switch ON the transformer. 
 + 
 +{{:crystallography:collection:frx:main_power_supply.jpg?600|}} 
 + 
 +Reset and then switch ON the generator at the back. 
 + 
 +{{:crystallography:collection:frx:frx_back.jpg?400|}} 
 + 
 +POWER ON on the front main panel. 
 +Press both DOOR LOCK buttons. 
 + 
 +{{:crystallography:collection:frx:frx_front.jpg?600|}}
  
 Start the Vacuum on the XG Control panel.  Start the Vacuum on the XG Control panel. 
 Wait until vacuum is below 1.10E-4 (about 1h30). Wait until vacuum is below 1.10E-4 (about 1h30).
 +
 +{{:crystallography:collection:frx:xg.png?600|}}
  
 Turn X-Rays ON on the XG Control panel. Turn X-Rays ON on the XG Control panel.
-Wait 1-2h if it was down for a few hours (heating with generate gaz that may disrupt the vacuum if the level is not low enough). Wait overnight if it was down for a few weeks.+Wait 1-2h if it was down for a few hours (heating will generate gaz that may disrupt the vacuum if the level is not low enough). Wait overnight if it was down for a few weeks.
  
 Start the AGING procedure. Start the AGING procedure.
-Short lasts 31 min. Then wait 1h30 for the beam to stabilize before data collection+Short aging lasts 31 min, long aging lasts 6h 
-Long lasts 6h.+Wait 1h30 for the beam to stabilize before data collection.
  
 ---- ----
  
 ==== Cryostream ==== ==== Cryostream ====
 +
 +Switch ON the helium compressor.
 +
 +{{:crystallography:collection:frx:helium.jpg?300|}}
 +{{:crystallography:collection:frx:helium_back.jpg?250|}}
  
 Switch ON on the back of the device. Switch ON on the back of the device.
 +
 +{{:crystallography:collection:frx:cobra_back.jpg?600|}}
  
 Cycle Start/Start Cycle Start/Start
Line 45: Line 88:
 Final temperature should be around 100 K. Final temperature should be around 100 K.
  
 +{{:crystallography:collection:frx:cobra_front.jpg?600|}}
 +
 +----
 +
 +==== Detector ====
 +
 +Switch ON the EIGER water chiller.
 +
 +{{:crystallography:collection:frx:eiger_chiller.jpg?400|}}
 +
 +Switch ON the power supply for the EIGER.
 +
 +{{:crystallography:collection:frx:eiger_power_supply.jpg?600|}}
 +
 +Switch ON the framegrabber.
 +
 +{{:crystallography:collection:frx:framegrabber.jpg?600|}}
  
crystallography/collection/frx/on.1469440101.txt.gz · Last modified: (external edit)