crystallography:collection:frx:on
Differences
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| Both sides previous revisionPrevious revisionNext revision | Previous revision | ||
| crystallography:collection:frx:on [2016/07/25 09:48] – bonnefon | crystallography:collection:frx:on [2023/11/01 20:19] (current) – external edit 127.0.0.1 | ||
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| Turn ON FR-X | Turn ON FR-X | ||
| - | ===== Turn in-house FR-X OFF ===== | + | ===== Turn in-house FR-X ON ===== |
| ---- | ---- | ||
| - | ==== Engine | + | ==== Technical |
| - | Switch ON the main switch of the water cooling device in the engine room. | + | Turn the tap on the main water inlet to the ON position. |
| + | |||
| + | {{: | ||
| + | |||
| + | Switch ON the water chiller (HASKRIS) using the main switch only. | ||
| Wait until the temperature is stabilized at 17°C. | Wait until the temperature is stabilized at 17°C. | ||
| + | {{: | ||
| + | {{: | ||
| - | Switch ON the nitrogen compressor | + | Switch ON the nitrogen compressor |
| After a 3 min idle wait, the pump should stabilize in 30 min. | After a 3 min idle wait, the pump should stabilize in 30 min. | ||
| - | Wait for 1 h. | + | Wait for 1 h. |
| + | |||
| + | {{: | ||
| + | {{: | ||
| ---- | ---- | ||
| Line 19: | Line 28: | ||
| ==== FR-X ==== | ==== FR-X ==== | ||
| - | Switch | + | Switch ON the two fans of AFC-11. |
| - | Reset and then switch ON at the back of the FR-X. | + | {{: |
| - | POWER ON on the FR-X main panel. | + | Switch ON AFC-11 Goniometer controller. |
| + | |||
| + | {{: | ||
| + | |||
| + | Switch ON the vacuum pump below the Cobra Controller. | ||
| + | |||
| + | {{: | ||
| + | {{: | ||
| + | |||
| + | Switch ON the vacuum pump below the BioSAXS. | ||
| + | |||
| + | {{: | ||
| + | {{: | ||
| + | |||
| + | Switch ON the transformer. | ||
| + | |||
| + | {{: | ||
| + | |||
| + | Reset and then switch ON the generator at the back. | ||
| + | |||
| + | {{: | ||
| + | |||
| + | POWER ON on the front main panel. | ||
| + | Press both DOOR LOCK buttons. | ||
| + | |||
| + | {{: | ||
| Start the Vacuum on the XG Control panel. | Start the Vacuum on the XG Control panel. | ||
| Wait until vacuum is below 1.10E-4 (about 1h30). | Wait until vacuum is below 1.10E-4 (about 1h30). | ||
| + | |||
| + | {{: | ||
| Turn X-Rays ON on the XG Control panel. | Turn X-Rays ON on the XG Control panel. | ||
| - | Wait 1-2h if it was down for a few hours (heating | + | Wait 1-2h if it was down for a few hours (heating |
| Start the AGING procedure. | Start the AGING procedure. | ||
| - | Short lasts 31 min. Then wait 1h30 for the beam to stabilize before data collection. | + | Short aging lasts 31 min, long aging lasts 6h. |
| - | Long lasts 6h. | + | Wait 1h30 for the beam to stabilize before data collection. |
| ---- | ---- | ||
| ==== Cryostream ==== | ==== Cryostream ==== | ||
| + | |||
| + | Switch ON the helium compressor. | ||
| + | |||
| + | {{: | ||
| + | {{: | ||
| Switch ON on the back of the device. | Switch ON on the back of the device. | ||
| + | |||
| + | {{: | ||
| Cycle Start/Start | Cycle Start/Start | ||
| Line 45: | Line 88: | ||
| Final temperature should be around 100 K. | Final temperature should be around 100 K. | ||
| + | {{: | ||
| + | |||
| + | ---- | ||
| + | |||
| + | ==== Detector ==== | ||
| + | |||
| + | Switch ON the EIGER water chiller. | ||
| + | |||
| + | {{: | ||
| + | |||
| + | Switch ON the power supply for the EIGER. | ||
| + | |||
| + | {{: | ||
| + | |||
| + | Switch ON the framegrabber. | ||
| + | |||
| + | {{: | ||
crystallography/collection/frx/on.1469440101.txt.gz · Last modified: (external edit)
