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crystallography:collection:frx:on [2017/09/18 07:37] bonnefoncrystallography:collection:frx:on [2023/11/01 20:19] (current) – external edit 127.0.0.1
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 Turn ON FR-X Turn ON FR-X
  
-===== Turn in-house FR-X OFF =====+===== Turn in-house FR-X ON =====
  
 ---- ----
  
-==== Technical Room ====+==== Technical Room E0044 ====
  
 Turn the tap on the main water inlet to the ON position. Turn the tap on the main water inlet to the ON position.
  
-Switch ON the main switch of the water cooling device in the engine room.+{{:crystallography:collection:frx:red_valve.jpg?400|}} 
 + 
 +Switch ON the water chiller (HASKRIS) using the main switch only.
 Wait until the temperature is stabilized at 17°C. Wait until the temperature is stabilized at 17°C.
  
 +{{:crystallography:collection:frx:haskins.jpg?200|}}
 +{{:crystallography:collection:frx:haskins_closeup.jpg?400|}}
  
-Switch ON the nitrogen compressor in the technical room using the touch panel.+Switch ON the nitrogen compressor at the back, then start the nitrogen flow with the touch panel.
 After a 3 min idle wait, the pump should stabilize in 30 min. After a 3 min idle wait, the pump should stabilize in 30 min.
-Wait for 1 h. +Wait for 1 h. 
 + 
 +{{:crystallography:collection:frx:n2.jpg?150|}} 
 +{{:crystallography:collection:frx:n2_closeup.jpg?400|}} 
  
 ---- ----
Line 21: Line 28:
 ==== FR-X ==== ==== FR-X ====
  
-Switch the main power source ON.+Switch ON the two fans of AFC-11.
  
-Reset and then switch ON at the back of the FR-X.+{{:crystallography:collection:frx:acf11_back.jpg?400|}}
  
-POWER ON on the FR-X main panel.+Switch ON AFC-11 Goniometer controller. 
 + 
 +{{:crystallography:collection:frx:afc11_closeup.jpg?600|}} 
 + 
 +Switch ON the vacuum pump below the Cobra Controller. 
 + 
 +{{:crystallography:collection:frx:pump1.jpg?250|}} 
 +{{:crystallography:collection:frx:pump1_closeup.jpg?250|}} 
 + 
 +Switch ON the vacuum pump below the BioSAXS. 
 + 
 +{{:crystallography:collection:frx:pump2.jpg?250|}} 
 +{{:crystallography:collection:frx:pump2_closeup.jpg?350|}} 
 + 
 +Switch ON the transformer. 
 + 
 +{{:crystallography:collection:frx:main_power_supply.jpg?600|}} 
 + 
 +Reset and then switch ON the generator at the back. 
 + 
 +{{:crystallography:collection:frx:frx_back.jpg?400|}} 
 + 
 +POWER ON on the front main panel. 
 +Press both DOOR LOCK buttons. 
 + 
 +{{:crystallography:collection:frx:frx_front.jpg?600|}}
  
 Start the Vacuum on the XG Control panel.  Start the Vacuum on the XG Control panel. 
 Wait until vacuum is below 1.10E-4 (about 1h30). Wait until vacuum is below 1.10E-4 (about 1h30).
 +
 +{{:crystallography:collection:frx:xg.png?600|}}
  
 Turn X-Rays ON on the XG Control panel. Turn X-Rays ON on the XG Control panel.
-Wait 1-2h if it was down for a few hours (heating with generate gaz that may disrupt the vacuum if the level is not low enough). Wait overnight if it was down for a few weeks.+Wait 1-2h if it was down for a few hours (heating will generate gaz that may disrupt the vacuum if the level is not low enough). Wait overnight if it was down for a few weeks.
  
 Start the AGING procedure. Start the AGING procedure.
-Short lasts 31 min. Then wait 1h30 for the beam to stabilize before data collection+Short aging lasts 31 min, long aging lasts 6h 
-Long lasts 6h.+Wait 1h30 for the beam to stabilize before data collection.
  
 ---- ----
  
 ==== Cryostream ==== ==== Cryostream ====
 +
 +Switch ON the helium compressor.
 +
 +{{:crystallography:collection:frx:helium.jpg?300|}}
 +{{:crystallography:collection:frx:helium_back.jpg?250|}}
  
 Switch ON on the back of the device. Switch ON on the back of the device.
 +
 +{{:crystallography:collection:frx:cobra_back.jpg?600|}}
  
 Cycle Start/Start Cycle Start/Start
 For the first hour the temperature won't really decrease much. For the first hour the temperature won't really decrease much.
 Final temperature should be around 100 K. Final temperature should be around 100 K.
 +
 +{{:crystallography:collection:frx:cobra_front.jpg?600|}}
  
 ---- ----
Line 51: Line 94:
 ==== Detector ==== ==== Detector ====
  
 +Switch ON the EIGER water chiller.
 +
 +{{:crystallography:collection:frx:eiger_chiller.jpg?400|}}
 +
 +Switch ON the power supply for the EIGER.
 +
 +{{:crystallography:collection:frx:eiger_power_supply.jpg?600|}}
 +
 +Switch ON the framegrabber.
 +
 +{{:crystallography:collection:frx:framegrabber.jpg?600|}}
  
crystallography/collection/frx/on.1505720246.txt.gz · Last modified: (external edit)