Turn ON FR-X ===== Turn in-house FR-X ON ===== ---- ==== Technical Room E0044 ==== Turn the tap on the main water inlet to the ON position. {{:crystallography:collection:frx:red_valve.jpg?400|}} Switch ON the water chiller (HASKRIS) using the main switch only. Wait until the temperature is stabilized at 17°C. {{:crystallography:collection:frx:haskins.jpg?200|}} {{:crystallography:collection:frx:haskins_closeup.jpg?400|}} Switch ON the nitrogen compressor at the back, then start the nitrogen flow with the touch panel. After a 3 min idle wait, the pump should stabilize in 30 min. Wait for 1 h. {{:crystallography:collection:frx:n2.jpg?150|}} {{:crystallography:collection:frx:n2_closeup.jpg?400|}} ---- ==== FR-X ==== Switch ON the two fans of AFC-11. {{:crystallography:collection:frx:acf11_back.jpg?400|}} Switch ON AFC-11 Goniometer controller. {{:crystallography:collection:frx:afc11_closeup.jpg?600|}} Switch ON the vacuum pump below the Cobra Controller. {{:crystallography:collection:frx:pump1.jpg?250|}} {{:crystallography:collection:frx:pump1_closeup.jpg?250|}} Switch ON the vacuum pump below the BioSAXS. {{:crystallography:collection:frx:pump2.jpg?250|}} {{:crystallography:collection:frx:pump2_closeup.jpg?350|}} Switch ON the transformer. {{:crystallography:collection:frx:main_power_supply.jpg?600|}} Reset and then switch ON the generator at the back. {{:crystallography:collection:frx:frx_back.jpg?400|}} POWER ON on the front main panel. Press both DOOR LOCK buttons. {{:crystallography:collection:frx:frx_front.jpg?600|}} Start the Vacuum on the XG Control panel. Wait until vacuum is below 1.10E-4 (about 1h30). {{:crystallography:collection:frx:xg.png?600|}} Turn X-Rays ON on the XG Control panel. Wait 1-2h if it was down for a few hours (heating will generate gaz that may disrupt the vacuum if the level is not low enough). Wait overnight if it was down for a few weeks. Start the AGING procedure. Short aging lasts 31 min, long aging lasts 6h. Wait 1h30 for the beam to stabilize before data collection. ---- ==== Cryostream ==== Switch ON the helium compressor. {{:crystallography:collection:frx:helium.jpg?300|}} {{:crystallography:collection:frx:helium_back.jpg?250|}} Switch ON on the back of the device. {{:crystallography:collection:frx:cobra_back.jpg?600|}} Cycle Start/Start For the first hour the temperature won't really decrease much. Final temperature should be around 100 K. {{:crystallography:collection:frx:cobra_front.jpg?600|}} ---- ==== Detector ==== Switch ON the EIGER water chiller. {{:crystallography:collection:frx:eiger_chiller.jpg?400|}} Switch ON the power supply for the EIGER. {{:crystallography:collection:frx:eiger_power_supply.jpg?600|}} Switch ON the framegrabber. {{:crystallography:collection:frx:framegrabber.jpg?600|}}